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Упит dcterms_subject_txt:Influence of synthesis method

2847 items

  • Solid state synthesis of extra phase-pure Li4Ti5O12 spinel

    Ivana Veljković, Dejan Poleti, Ljiljana Karanović, Miodrag Zdujić, Goran Branković (2011)
    Фазно чист спинел Li4Ti5O12 са величином честица мањом од 500 nm добијен је реакцијом у чврстом стању из стехиометријске смеше наноанатаса (ТiО2) и Li2CO3 која је претходно активирана механохемијским поступком. Реакција у чврстом стању у потпуности се завршава за само 4 часа на температури од 800 ºC. Уз помоћ XRPD, SEM и TG/DSC анализе испитане су структурне и микроструктурне карактеристике добијеног спинела, механизам реакције између анатаса и Li2CO3, као и термичка стабилност Li4Ti5O12. Реакција започиње разлагањем Li2CO3 на температурама ...
    дифракција рендгенских зрака, механизам реакције, термичка стабилност, Li4Ti5O12, спинел, фазно чист узорак

  • Synthesis, characterization, biomolecular interactions, molecular docking, and in vitro and in vivo anticancer activities of novel ruthenium(III) Schiff base complexes

    Milica Međedović, Aleksandar Mijatović, Rada Baošić, Dejan Lazić, Žiko Milanović, Zoran Marković, Jelena Milovanović, Dragana Arsenijević, Bojana Stojanović, Miloš Arsenijević, Marija Milovanović, Biljana Petrović, Ana Rilak Simović (2023)
    In order to discover new anticancer drugs, novel ruthenium(III) complexes [Ru(L)Cl(H2O)], where L is tetradentate Schiff base bis(acetylacetone)ethylendiimine (acacen, 1), bis(benzoylacetone)ethylendiimine (bzacen, 2), (acetylacetone)(benzoylaceton)ethylendiimine (acacbzacen, 3), bis(acetylacetone)propylendiimine (acacpn, 4), bis(benzoylacetone)propylendiimine (bzacpn, 5) or (acetylacetone)(benzoylaceton)propylendiimine (acacbzacpn, 6), were synthesized. The complexes 1 – 6 were characterized by elemental analysis, molar conductometry, and by various spectroscopic techniques, such as UV–Vis, IR, EPR, and ESI-MS. Based on in vitro DNA/BSA experiments, complexes 2 (bzacen) and 5 (bzacpn) with two aromatic rings showed ...
    Inorganic Chemistry, Biochemistry

  • Synthesis, magnetic, thermal and structural properties of Co(II), Ni(II) and Cu(II) complexes containing isophthalato ligands

    Jelena Rogan, Dejan Poleti, Ljiljana Karanović, Zvonko Jagličić (2011)
    A series of novel ternary Co(II), Ni(II) and Cu(II) complexes containing 2,20-dipyridylamine (dipya), 2,20-bipyridine (bipy), and 1,10-phenanthroline (phen), as aromatic diamine ligands, and dianion of isophthalic acid (ipht) have been prepared by ligand exchange reactions from diluted H2O/EtOH solutions. The complexes were characterized by elemental analysis, IR spectroscopy, magnetic susceptibility measurements and TG and DSC analysis. Three complexes, Cu(dipya)(ipht)H2O (1), Co(dipya)(ipht)2H2O (2) and Cu(ipht)(phen)2H2O (5) are polymeric with bis-monodentate ipht, while the other two complexes M(bipy)(ipht)4H2O, M@Co(II) (3) and ...
    комплекси прелазних метала, карбоксилатни лиганди, N-лиганди, кристална структура, магнетна својства

  • The external aggregation Newton's method for solving nonlinear equations and applications

    Marija Paunović, Dejan Ćebić, Nebojša Ralević (2020)
    Њутнов метод, агрегациона функција, ред конвергенције

  • Application of Lignite Combustion Waste Slag Generated in Heating Plants as a Partial Replacement for Cement. Part II: Physical–Mechanical and Physical–Chemical Characterization of Mortar and Concrete

    Milan Kragović, Nenad Ristić , Jelena Gulicovski, Andrijana Nedeljković, Snežana Pašalić, Ivica Ristović, Marija Stojmenović (2021)
    sagorevanje lignita, otpadna šljaka, zamena cementa, proizvodnja maltera i betona, fizičko-mehanička i fizičko-hemijska karakterizacija
    ... Łaźniewska-Piekarczyk, B. Use of Slag from the Combustion of Solid Municipal Waste as a Partial Replacement of Cement in Mortar and Concrete. Materials 2020, 13, 1593. [CrossRef] 12. Rivera, J.F.; Cristelo, N.; Fernández-Jiménez, A.; de Gutiérrez, R.M. Synthesis of alkaline cements based on fly ash ...
    ... Enhancement of Mechanical and Thermal Properties of Polycaprolactone/Chitosan Blend by Calcium Carbonate Nanoparticles. Int. J. Mol. Sci. 2012, 13, 4508–4522. [CrossRef] [PubMed] Minerals 2021, 11, 925 16 of 16 30. Tran, T.N.; Pham, T.V.A.; Le, M.L.P.; Nguyen, T.P.T.; Tran, V.M. Synthesis of amorphous ...
    ... Sengül, K.; Erdogan, S.T. Influence of ground perlite on the hydration and strength develop-ment of calcium aluminate cement mortars. Constr. Build. Mater. 2021, 266, 120943. [CrossRef] 27. Mojet, B.L.; Ebbesenz, S.D.; Lefferts, L. Light at the interface: The potential of attenuated total reflection ...

  • Life Cycle Assessment of Individual Wood Biomass Heating Systems in Households

    Boban Pavlović, Dejan Ivezić, Marija Živković (2020)
    The use of solid fuels (wood biomass and coal) for heating of households continues to be common practice within European countries. Solid fuel combustion in households contributes more than 46% to total emissions of fine particulate matter. In this study, a life-cycle assessment (LCA) of firewood-based and pellet-based heating systems is performed. These two systems represent two different types of individual wood biomass heating systems. In the case of the firewood-based heating systems, it is analyzed a typical stove ...
    Grejanje, Analiza životnog ciklusa, Drvna biomasa, Individualni sistemi grejanja
    ... (2014). Synthesis Report. Contribution of Working Groups I, II and III to the Fifth Assessment Report of the IPCC, IPCC, Geneva, Switzerland.https://www.ipcc.ch/site/assets/uploads/2018/05/SYR_AR5_FINAL_full _wcover.pdf (accessed 30 Sep. 2020). [17] AERS, Energy Agency of the Republic of Serbia (2018) ...
    ... same time, it ensures the financial benefits through savings and conservation of natural resources. This research showed that the implementation of LCA for assessing heating systems is an efficient and relatively simple method for obtaining new information regarding the household heating sector. Key ...
    ... continual improvement of its environmental performance. Boban Pavlović, Dejan Ivezić. Marija Živković 430 However, since LCA considers the environmental aspects and the potential impacts of a product or a service system throughout its life, it becomes a very useful method for researching studies ...

  • Microstructural and magnetic properties of electrospun hematite/cuprospinel composites

    Mira Ristić, Aleksandar Kremenović, Michael Reissner, Željka Petrović, Svetozar Musić (2020)
    Phase composition, microstructural and magnetic properties of electrospun hematite/cuprospinel composites were investigated. Samples were synthesized starting with 0 to 10 mol% of copper relative to iron. The round shape of reference electrospun fbres was preserved upon their heating up to 600 °C in air, whereas at 700 °C hollow substructure was additionally formed. In these reference samples the presence of hematite phase was detected by XRPD. A small amount (traces) of Fe3O4 /γ-Fe2O3 was also found, due to the ...
    Electrical and Electronic Engineering, Condensed Matter Physics, Atomic and Molecular Physics and Optics, Electronic, Optical and Magnetic Materials

  • Three new Sr-bearing arsenates, hydrothermally synthesized in the system SrO–MO–As2O5–H2O (M2+ = Mg, Cu, Zn)

    Tamara Đorđević, Ljiljana Karanović (2018)
    During systematic research on the mineral-related synthetic arsenates, with particular focus on their structural and spectroscopic classification, three new Sr-containing arsenates Sr2Mg(AsO4)2· 2H2O (1), Sr2Zn4(AsO4)4·H2O (2) and Sr2Cu7(AsO4)6 (3) have been synthesized under low-temperature hydrothermal conditions in the system SrO MO As2O5 H2O (M 2þ = Mg, Zn, Cu). Their crystal structures were determined using room-temperature single-crystal X-ray diffraction data and refined to the following R-values: 1– R1 = 0.025; 2– R1 = 0.030; 3– R1 = 0.035. Compounds ...
    стронцијум, арсен, арсенати, кристална структура, дифракција рендгенских зрака на монокристалима, хидротермална синтеза, Раманска спектроскопија

  • Natural two-dimensional pyrophyllite: Nanoscale lubricant, electrical insulator and easily-machinable material

    Borislav Vasić, Radoš Gajić, Ivana Milošević, Žarko Medić, Marina Blagojev, Marko Opačić, Aleksandar Kremenović, Dejan Lazić (2022)
    Pyrophyllite, with the chemical formula Al2Si4O10(OH)2, is a naturally occurring and abundant van der Waals mineral belonging to the group of phyllosilicates. It is very soft, layered crystal used for sculpting and an excellent electrical and thermal insulator aimed for the operation at high pressure and temperature. Here, for the first time, two-dimensional (2D) pyrophyllite obtained by both mechanical and liquid phase exfoliation is presented and investigated at the nanoscale. The layered structure provides low friction coefficient of around ...
    Atomic force microscopy, Insulating properties, Nanofriction and wear, Natural two dimensional materials, Phyllosilicates, Pyrophyllite

  • A Fuzzy Expert Model for Availability Evaluation

    Dejan Ivezić, Miloš Tanasijević, Predrag Jovančić, Radiša Đurić (2019)
    Each technical system within itself carries the great potential danger of possible occurrence of failure and damages. Mining machines are characteristic by great investment values, costs of unplanned shutdowns, complex working conditions, and environment and workers hazards. Systematic monitoring of the mining machinery is of great importance for the management of the mining companies. Availability is the overall concept of quality of service. Includes information regard to operating state, an idle state, a standby state and shut down. The ...
    raspoloživost, ekspertski sistem, fazi teorija, buldozeri
    ... USA [7] Kabir S., Papadopoulos Y., A review of applications of fuzzy sets to safety and reliability engineering, International Journal of Approximate Reasoning, Vol. 100, Pages 29-55, 2018. [8] Wang, J., Yang, J.B., Sen, P. Safety analyses and synthesis using fuzzy sets and evidential reasoning. ...
    ... and quality of service. Availability performance has a decisive influence on the dependability and the quality of service due to the known fact that the machine must be primarily available for operation in order to obtain performance. The achievement of the satisfactory value of the machine's ...
    ... combination represents one possible input for synthesis and evaluation of A. Ac = [μR j=1, …, n, μM j=1, …, n ,…, μS j=1, …, n] , for all c = 1 to C (2) If only values of µR,M,S j = 1, …, 5 ≠ 0 are taken into consideration, o outcomes (o = 1 to O, where O˂=C) are obtained. Additionally ...

  • Mean-based iterative methods for finding multiple roots in nonlinear chemistry problems

    Dejan Ćebić, Nebojša M. Ralević (2021)
    нелинеарне једначине, поступци засновани на срединама, вишеструки корени,

  • Синтеза и карактеризација керамике на бази сфена

    Jelena R. Pantić (2015-07-10)
    Механохемијска активација стехиометријске смеше реактаната TiO2, SiO2 и CaCO3 показала се као веома успешна и једноставна метода за добијање сфена (CaTiSiO5). На основу мерења релативних густина свих синтерованих узорака установљено је да максималну густину од 93,9 % имају узорци који су активирани 30 минута и синтеровани на 1200 °С. Микроструктурном анализом, тј. анализом слика синтерованих узорака активираних 30 минута, које су добијене скенирајућом електронском микроскопијом, опажа се бимодална расподела величине зрна, са просечном величином од 3 μm, односно 5 ...
    сфен, механохемија, Ритвелдова метода, оптичка спектроскопија, микроструктурна анализа, фазна трансфоpмација, чврсти раствори
    ... A.; Kremenović, A.; Mihovil Logar, M.: „Influence of mechanical activation of sphene ceramic synthesis”, VII International Conference on Mechanochemistry and Mechanical Alloying INCOME 2011, August 31-September 3, 2011, Herceg Novi, Montenegro, Book of abstracts, 52 2. Pantić, J.; Prekajski ...
    ... Baščarević Z., Matović B. (2013) Influence of mechanical activation on sphene based ceramic material synthesis. Ceram Inter 39: 1483-1488. Pantić J., Prekajski M., Dramićanin М., Abazović N., Vuković N., Kremenović A., Matović B. (2013) Preparation and characterization of chrome doped sphene pigments ...
    ... Z.; Matović, B.: „Influence of mechanical activation on sphene based ceramic material synthesis”, Ceram Int 39 [1] (2013) 483-488. 2. Pantić, J.; Prekajski, M.; Dramićanin, M.; Abazović, N.; Vuković, N.; Kremenović, A.; Branko Matović, B.: „Preparation and characterization of chrome doped sphene ...

  • Синтеза и карактеризација керамике на бази сфена

    Jelena R. Pantić (2015-07-10)
    Механохемијска активација стехиометријске смеше реактаната TiO2, SiO2 и CaCO3 показала се као веома успешна и једноставна метода за добијање сфена (CaTiSiO5). На основу мерења релативних густина свих синтерованих узорака установљено је да максималну густину од 93,9 % имају узорци који су активирани 30 минута и синтеровани на 1200 °С. Микроструктурном анализом, тј. анализом слика синтерованих узорака активираних 30 минута, које су добијене скенирајућом електронском микроскопијом, опажа се бимодална расподела величине зрна, са просечном величином од 3 μm, односно 5 ...
    сфен, механохемија, Ритвелдова метода, оптичка спектроскопија, микроструктурна анализа, фазна трансфоpмација, чврсти раствори
    ... A.; Kremenović, A.; Mihovil Logar, M.: „Influence of mechanical activation of sphene ceramic synthesis”, VII International Conference on Mechanochemistry and Mechanical Alloying INCOME 2011, August 31-September 3, 2011, Herceg Novi, Montenegro, Book of abstracts, 52 2. Pantić, J.; Prekajski ...
    ... Baščarević Z., Matović B. (2013) Influence of mechanical activation on sphene based ceramic material synthesis. Ceram Inter 39: 1483-1488. Pantić J., Prekajski M., Dramićanin М., Abazović N., Vuković N., Kremenović A., Matović B. (2013) Preparation and characterization of chrome doped sphene pigments ...
    ... Z.; Matović, B.: „Influence of mechanical activation on sphene based ceramic material synthesis”, Ceram Int 39 [1] (2013) 483-488. 2. Pantić, J.; Prekajski, M.; Dramićanin, M.; Abazović, N.; Vuković, N.; Kremenović, A.; Branko Matović, B.: „Preparation and characterization of chrome doped sphene ...

  • Analysis Of the Process Of Carbon Capture Utilization And Storage In Underground Reservoirs

    John Nyame (2024)
    The importance of mitigating the effects of global climate change has necessitated an in-depth exploration of innovative strategies to reduce carbon dioxide (CO2) emissions. Among these strategies, Carbon Capture, Utilization, and Storage (CCUS) has emerged as a promising and transformative solution. This master thesis delves into the diverse realm of CCUS processes, aiming to unravel the positives challenges, and opportunities within this dynamic field. The analysis begins with a systematic examination of carbon capture technologies, encompassing post-combustion, pre-combustion, and oxy-fuel combustion ...
    Carbon Capture, Utilization and Storage
    ... feedstock for the synthesis of ammonia and chlorine. The hydrate-forming method is another technique that is used for desalination, and it involves the formation of hydrates by using CO2 to separate the salts from water [16]. A challenge with the desalination process is the waste of brine solids in ...
    ... include a range of —10.5 to +10.5 USS/t CO- stored for European sites. Cost estimates show that CO»-enhanced gas recovery can provide a benefit of 4-16 USS/t COx, depending on the price of gas and the effectiveness of recovery [61]. Figure 4.5 shows an enhanced oil recovery method used to store CO» ...
    ... p8832-8849 [75] Zhang, L. et al.: The integration of hydrogenation and carbon capture utilization and storage technology: A potential low-carbon approach to chemical synthesis in China. 2021. p4-12. DOI: 10.1002/er.7076 [76] Junwen Z. Study on test of displacement coal-bed methane by carbon dioxide ...

  • Multi-Criteria Approach for Selecting Optimal Dozer Type in Open-Cast Coal Mining

    Ivan Janković, Stevan Đenadić , Dragan Ignjatović , Predrag Jovančić , Tomislav Šubaranović, Ivica Ristović (2019)
    Analitički hijererhijski proces (AHP), dozeri, eksploatacija uglja, površinski kopovi
    ... application of the AHP method as one of the most used method of multicriteria decision analysis (MDCA) showed the rank of different types of dozer most commonly used auxiliary machine in open-cast coal mine of Kolubara. The subjects of the analysis were four dozers analysed by a combination of four basic ...
    ... schematic display of the structure of the analytical hierarchy process (AHP) method. The mathematical basis of the AHP method consists of four steps: 1. Production of a hierarchical model, that is, the structure of the decision-making problem (presented in Figure 2); 2. The use of an appropriate Saaty ...
    ... subject of interest is not the exact measurements of separate quantities but the proportional relationship that exists among them. It is based on three main principles [30]: Identity and decomposition, the comparison of pairs, and the synthesis of priorities. Energies 2019, 12, 2245 4 of 16 Energies ...

  • The interaction of organoselenium trans-palladium(II) complexes toward small-biomolecules and CT-DNA

    Vera M. Divac, Aleksandar Mijatović, Marina D. Kostić, Jovana Bogojeski (2017)
    Serija organoselenijum trans-paladijum(II) kompleksa 1 (bis(2-(fenilselanilmetil)oksolan)dihloropaladijum(II)), 2 (bis(2-(fenilselanilmetil)oksan)dihloropaladijum(II)) i 3 (bis(2) ,2-dimetil-3-(fenilselanil)oksan)dihloropaladijum(II)) su korišćeni za ispitivanje reaktivnosti ovog specifičnog tipa kompleksa prema različitim bio-molekulima. Ovaj sistem je od posebnog interesa jer se jako malo zna o supstitucionim reakcijam organoselenijum paladijum(II) kompleksa sa trans konfiguracijom. Zamena koordinovanog hlorida sa serijom malih bio-molekula (l-Met, l-His, l-Cis, GSH i 5′-GMP) proučavana je pod uslovima pseudo-prvog reda kao funkcija koncentracije nukleofila i temperature korišćenjem tehnika zaustavljenog toka. Rezultati za proučavane komplekse ukazuju da ...
    Pd(II), Selen, Substitucija, Kinetika, Mehanizam

  • Overcoming the Low Oral Bioavailability of Deuterated Pyrazoloquinolinone Ligand DK-I-60-3 by Nanonization: A Knowledge-Based Approach

    Jelena R. Mitrović , Branka Divović-Matović, Daniel E. Knutson, Jelena B. Ðoković, Aleksandar Kremenović, Vladimir D. Dobričić, Danijela V. Randjelović, Ivana Pantelić, James M. Cook, Miroslav M. Savić, Snežana D. Savić (2021)
    Poor water solubility of new chemical entities is considered as one of the main obstacles in drug development, as it usually leads to low bioavailability after administration. To overcome these problems, the selection of the appropriate formulation technology needs to be based on the physicochemical properties of the drug and introduced in the early stages of drug research. One example of the new potential drug substance with poor solubility is DK-I-60-3, deuterated pyrazoloquinolinone, designed for the treatment of various neuropsychiatric ...
    pyrazoloquinolinones, nanocrystals, wet media milling, fasted/fed bioavailability
    ... 12 ± 0.07 µg/mL) [27]. The particle size of nanocrystals in the dialysis bag after the experiment did not change (p > 0.05, Student t-test, Table S2), confirming the strong influence of dialysis membrane on dissolution. Therefore, the dialysis membrane method most probably did not give a true release ...
    ... 4 h, and 8 h), 1 mL of medium with dissolved particles was withdrawn and replaced with 1 mL of fresh medium. The experiments were performed in triplicate, and the concentration of DK-I-60-3 in samples was analyzed by the LC-MS/MS method. Solubility of Nanocrystals Solubility of nanocrystals in formulations ...
    ... non-benzodiazepine ligands to interact with α6β2/3γ2 subunit of GABAA receptors with improved metabolic stability to retard O-demethylation. Deuteration of both C4′ and C7′ methoxy groups in the parent molecule resulted in the synthesis of the ligand DK-I-60-3 (7-Methoxy-d3-2-(4-methoxy- d3-phenyl)-2 ...

  • Development Of The Serbian Geological Resources Portal

    Ranka Stanković, Jelena Prodanović, Olivera Kitanović, Velizar Nikolić (2011)
    ... geodiversity of North-Western Serbia. 9 The project was funded by MEMSP, Geologic Institute of Serbia: Geo-heritage and geo-diversity of North-Western Serbia 2007-2011, FILIPOVIĆ, I. & JOVANOVIĆ, D. 2011. FMG: Synthesis of geological research of jewelry mineral resources of Serbia with the evaluation of potential ...
    ... entered, the method on the server sums up the number of appear- ances of the word “gold” in the abovementioned fields in relation to the given factor. Ranking of the results is carried out in descending order according to the field containing the total sum of factors. The search method described here ...
    ... Projects funded by MEMSP. FMG: Geological bibliography of the Republic of Serbia the ranking of search results, based of the number of appearances of a key word or phrase, and the sum of weigh factors of the search field. Namely, a number of entities and their attributes within the database corre- ...

  • Tl(I) sequestration by pharmacosiderite supergroup arsenates: synthesis, crystal structures and relationships in Tl(I)–M(III)–As(V)–H2O (M = Al, Fe) system

    Tamara Đorđević, Tarik Karasalihović, Michael Stöger-Pollach, Ljiljana Karanović (2023)
    talijum, farmakosideritna supergrupa arsenata, talijumfarmakosiderit

  • Structural dissymmetrization of optically anisotropic Grs64±1Adr36±1Sps2 grandite from Meka Presedla (Kopaonik Mt., Serbia)

    Pavle Tančić, Aleksandar Kremenović, Predrag Vulić (2019)
    In this paper, grandite core with Grs64±1Adr36±1Sps2composition was crystallographically studied. This core represents zone A of the macroscopically visiblefive A–E zones of the optically anisotropic Grs58–64 Adr36–42Sps2 grandite. The applied procedure includes the detailed analysis of the powder diffraction patterns, and the Rietveld refinements of the crystal structures in a series of 18 space groups and two mixtures, which were followed by the comparative analysis of the R-values, site occupancy factors, and the bond lengths and angles. Synthesis of all ...
    grandite, XRPD, crystal structure, structural dissymmetrization